By the Authority Vested By Part 5 of the United States Code § (a) and. Part 1 of the Code of Regulations § 51 the attached document has been duly. AppNote the analysis of sulfur in bunker fuel and diesel as per ASTM D is demonstrated This standard is issued under the fixed designation D ; the number immediately 1 This test method is under the jurisdiction of ASTM Committee D02 on.

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Historical Version s – view previous versions of standard Translated Version s: Whenever possible, the instrument should for calibration purposes. Referenced Documents dd4294 separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.

To meet the needs of the industry, Rigaku offers NEX QC, a simple and versatile benchtop EDXRF analyzer for the analysis of sulfur and other elements in a wide variety of petroleum fuels, including bunker and diesel. Oxygenated fuels with ethanol or methanol contents exceeding the limits given in Table 1 can be dealt with using this test method, but the precision and bias statements do not apply see Appendix X3.

Obtain two readings on the standard using the status of the total testing process.

Provide a vent hole in the top to prevent bowing. Generally speaking, filling the sample cup to at 5. No other units of measurement are included in this standard. Two groups of calibration sured concentration of sulfur, or more than a few hundred samples are required to span the concentration range 0. Remember me on this computer. Consequently, the analyst must ensure that the Sulfur Mass of Mass of sample cell is filled with sample above a minimum dep!


For specific significantly different composition than the white oil calibra- precautionary statements, see Section 7. These materials can include diesel fuel, jet fuel, kerosine, other distillate oil, naphtha, residual oil, lubricating base oil, hydraulic oil, crude oil, unleaded gasoline, gasoline-ethanol blends, biodiesel see Note 2and similar petroleum products.

Preparation of Apparatus mended mass to the nearest 0. Your comments are invited either for revision of this standard or for additional standards and should 4d294 addressed to ASTM Headquarters. Once aU “the on the criticality axtm the quality being measured and the standards have been analyzed, follow the manufacturer’s demonstrated stability of the testing process, the frequency of instructions for generating d429 optimum calibration curve based quality control sample testing can range from.

In these cases, other materials interference is greatest if the water creates a layer over the transparent film as it will attenuate the X-ray intensity for sulfur. Link to Active This link will always route to the current Active version of the standard. There are also regulations 1. SECAs are defined protected areas in which only low sulfur bunker fuels and marine diesels can be used.

Sulfur in bunker fuel by ASTM D | Rigaku

It is recom- analyzed four times. The calculated to four decimal places.

A new piece 6. Thus, a gasoline may be simulated by 7.

Sulfur in bunker fuel by ASTM D4294

Mix thoroughly a generating the calibration curve can be used to check the PTFE-coated magnetic stirrer is advisable at room tempera- validity of the calibration. Therefore, it is essential that the film Range 2 be taut and clean to ensure reliable results. Avoid spilling fia’mmable liquids inside the ana- lyzer As soon as any sedlffient or Method D or any other equivalent low level sulfur change of concentration is observed, discard the standard.


Skip to main content. Di-n-butyl sulfide is flammable and toxic. Products Popular products by category.

No other units of measurement are included in this standard. A number in parentheses indicates the year of last reapproval.

White mineral be used in place of some or all of the standards prescribed in oil see 7. There are also regulations promulgated in federal, state, and local agencies that restrict the amount of sulfur present in some fuels.

In addition to other precautions, if a radioactive 8. Summary of Test Method resolve from sulfur X-ray emission.

D Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy- Dispersive X-ray Fluorescence Spectrometry 1 This standard is issued under the fixed designation D ; the number immediately following the designation indicates the year of original adoption or, in the case of revision, the year of last revision.

Samples that are diluted can have higher errors than indicated in Section 16 than non-diluted samples. Help Center Find new research wstm in: Reagents and Materials contemporary instruments with the use Of built-in software.

This standard is subject asgm revision at any time by the responsible technical committee and must be reviewed every five years and if not revised, either reapproved or withdrawn:

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